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Prepare the following as directed.

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(a) ethane from ethene

When ethene reacts with hydrogen in the presence of Ni at 250 to 300 °C ethane is formed.

                         Ni

   H2C=CH2   +   H2             H3C-CH3

                        250-300°C

(b) Acetylene from tetra-halide

When an alkyl tetra-halide is heated with zinc dust, the elimination of halogen atoms takes place and acetylene is formed.

  Cl  Cl

H-C―C-H        +2Zn(dust)     heat           HC≡CH   +  2ZnCI2 Cl    

  Cl   Cl                                    (Ethyne)

(c) Carbon tetra-chloride from methane

  Alkanes react fairly with halogens in diffused sunlight only. CH4 reacts with Cl2 in diffused sun light to form chloromethane, dichloromethane tri chloromethane and finally Tetrachloromethane

                                        diffused

CH4      +     C12               CH3C1   +   HC1

                                Sunlight                Chloromethane

                                                  

CH3C1 +    C12                        CH2C12 +    HC1

                                                Dichloromethane

CH2C12 +   C12                        CHCl3   +    HCl

                                                Trichloromethane

                                                (Chloroform)

    

CHC13 +   C12                         CCl4    +    HC1

                                               Tetrachloromethane

                                               (Carbon tetrachloride)

 (d) Ethylene glycol from ethene

When ethene is treated with aq. alkaline KMn04 solution, ethylene glycol is formed in cold state.

 3CH2 = CH2   + 2KMnO4 +   4H2O         3CH2 ― CH2   +   2KMnO4   + 2KOH

(e)  1,2-dibromoethane from ethene

When ethene is treated with bromine 1, 2-dibromoethane is formed.

        H2C=CH2 + Br2 + Br-CH2-CH2-Br

(f) glyoxal from acetylene

When acetylene is oxidized by alkaline KMn04 hydroxyl groups add to triple bond. This intermediate product eliminates water molecules to form glyoxal.

HC≡CH   +   2KMnO   +   2H20   OH OH   +   2MnO2   +   2KOH

                                      H-C—C-H

                                          OH OH

                                             O O

   OH OH   -2H2O         ║ ║

  H-C—C-H                             H-C-C-H

OH OH                                  Glyoxal
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